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1 article(s) from Wang, Haopei

A photochemical C=C cleavage process: toward access to backbone N-formyl peptides

Haopei Wang and
Zachary T. Ball

Beilstein J. Org. Chem. 2021, 17, 2932–2938, doi:10.3762/bjoc.17.202

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Figure 1: Uncaging of peptide backbone N–H bonds from Chan–Lam-type modification.

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Figure 2: Photocleavage of compounds 1 and 6 under basic conditions. Yield of products was calculated from cr...

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Figure 3: (a) Photocleavage of compound 6 under acidic conditions. Yields determined by ¹H NMR using residual...

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Figure 4: Preparation and hydrolysis kinetics (inset) of N-formyl product 11. Dashed line: first-order decay ...

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Figure 5: Proposed mechanism for the formation of aldehyde 3 and N-formyl product 8.

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Letter

Published 15 Dec 2021

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